Aspirin synthesis lab quiz honors chemistry 2 with sparks at mattoon high school studyblue flashcards. In fact, its better to use more water than they usually say for recrystallization of aspirin to avoid oiling out. The purpose of this experiment is to calculate the percent yield of aspirin synthesized in the lab. Casey goettel march 19, 2015 organic chemistry ii section 21 introduction purpose the purpose of this experiment is to synthesize and analyze aspirin by the esterification of salicylic acid to aspirin using acetic anhydride. After recrystallisation differences between the crude and purified aspirin were noted.
In the presence of moisture, aspirin may decompose hydrolysis into salicylic acid and acetic acid. Synthesis and spectral analysis of aspirin synthesis and. Later it was demonstrated that salicylic acid and its derivatives organic compounds called salicylates affected the production of prostaglandins. Currently in depth estimation reference software 6. The aspirin content of the three tablets analysed are given in table 2. Using bibliographic software to record and manage references will help in. Depth estimation and view synthesis for immersive media. Analytical method development and validation for aspirin. The development of the onehealth software and manual was supported by the world health. Mpegi depth estimation reference software semantic scholar. Depth estimation and view synthesis for narrowbaseline.
Title informative title for lab report, your name, lab partners name, and section number. Start studying synthesis and analysis of aspirin lab. If youre talking about the recrystallization, the wrong temperatures can result in impure product, loss of product, and oiling out. The quantitative determination of the aspirin content of tablets using uv and visible wavelength spectroscopy introduction since its market introduction in 1899 under the. In the present investigation hydrotropic solubilization technique has been employed to solubilize poorly watersoluble aspirin analgesic and antipyretic drug by 0. I need to prepare aspirin for my school chemistry project but the school board bans the use of acetic anhydride. The synthesis and characterization of aspirin part 1. The purity of the product is tested using the melting point, thin layer. The purity of the product will be confirmed by measuring its melting point range. Isoiec jtc1sc29wg11, reference softwares for depth estimation and view synthesis, doc. Concept note for estimating costs of country health information systems. Studies of different types of aspirin by spectrophotometric. Our main idea is to synthesize a new virtual view from each of reference views. This is the second of two weeks related to aspirin.
Synthesis of aspirin performs the synthesis of acetylsalicylic acid aspirin purification by recrystallization and using melting point to confirm identity. Experiment 11 synthesis and analysis of aspirin introduction aspirin is most widely sold overthecounter drug. A novel smoothness energy term is proposed to enforce powerful smoothness of the estimated depth. It is known from the nmr spectrum of acetone, which is a reference compound with only one type of hydrogen that belonging to ch 3, that the peak at 2 ppm in the acetic acid spectrum pertains to ch 3 table 2. To synthesize acetylsalicylic acid aspirin, purify it, and determine the percent yield. In 3d warping, pixels in reference image are backprojected to 3d spaces, and reprojected onto the target viewpoint as shown in fig. Learn vocabulary, terms, and more with flashcards, games, and other study tools. Literature survey suggest that there are analytical method by hplc for the estimation of aspirin, but the reported method for aspirin estimation have some. Nagoya university tanimoto laboratory provides the depth estimation software and view synthesis software as the reference software for the ee on 3dv of mpegftv.
Yes, you can use hcl and hno3 but these are rather harsher acid and can cause decomposition or side products in your reaction. From that 20 ml is pipette, acidified with 2 ml con. By default ders requires 3 views for depth estimation. Synthesis and recrystallization of aspirin trial 1 mass of salicylic acid g 2. Jan 25, 2018 aspirin synthesis tap water was heated on a steam bath in a 250 ml beaker. Cuza university iasi, 11 carol i bd, iasi 700506, romania abstract. Abstract the abstract is a complete, but concise summary of the research. Enhanced depth estimation reference software ders for freeviewpoint. Minimumvalueofdisparitysearchrange, maximumvalueofdisparitysearchrange. Aspirin synthesis and characterization lab report aspirin. The last is conducting a colorimetric analysis on the aspirin sample.
Synthesis of aspirin in the first part of the experiment, aspirin was synthesized. Remote work advice from the largest allremote company. Aspirin synthesis formal lab report by dane brown on prezi. Add 5 ml of 1 m sodium hydroxide and carefully heat the mixture until all solid dissolves. In this experiment, you will measure the melting point of your synthesized asa product, salicylic acid, a crushed aspirin tablet, and pure asa from a manufacturer. Nagoya university tanimoto laboratory provides the depth estimation software and view synthesis software as the reference software for the ee on 3dv of. Percentage yield is worked out by actual yield of synthesised aspirin. Choose from 112 different sets of aspirin synthesis flashcards on quizlet. Enhanced depth estimation reference software ders for.
When salicylic acid reacts with acetic anhydride in the presence of an acid catalyst, acetylsalicylic acid, or aspirin, is produced according to the following equation. Then add 50 ml of brominating mixture, shake well for 15min. Jan 04, 2009 basically, sulfuric acid is used as an acid catalyst. Since the light field images are compatible to the multi view images, we are investigating a decimated multi view coding method using mpeg depth estimation reference software ders and view synthesis reference software vsrs. This reaction is the reverse of the synthesis reaction. Place approximately 200 ml of water into a 400 ml beaker and allow to warm to 70c on a hot plate further analysis when was aspirin first synthesized, by whom, and for what purpose. The existing ders has been refactored, debugged and extended to any number of input views for generating accurate depth maps. Results and conclusion for aspirin synthesis essay medicine. The temperature of an alcohol thermometer was equilibrated in a beaker of room temperature tap water.
Experimental results show a significant improvement of the initial input depth maps and coding efficiency, as well as a reduction of view synthesis artifacts. Postu department of chemistry, american university, washington, d. Lc method development and validation of aspirin and. Then 40 ml 10% naoh is added and refluxed for 15 min. Transfer the solution quantitatively into a 250 ml standard flask, made upto the mark. Studies of different types of aspirin by spectrophotometric methods gabriela motan,a aurel puia adepartment of chemistry, al. Synthesis of aspirin lab report essay example for free newyorkessays database with more than 65000 college essays for studying. The views expressed in this publication are those of crd and not. Reference softwares for depth estimation and view synthesis. In vitro, aspirin diminished cellular oxygen free radicals ros, nitric oxide no. It results from the elimination of a molecule of water from two molecules of acetic acid see fig. The software and data of this site can be used only for the purpose of ee by the participants in the ee on 3dv of mpegftv. Depth estimation is performed by global energy minimization using graph cut technique. Quantitative determination of acetylsalicylic acid in aspirin.
The method was specific since excipients in the formulation did not interfere in the estimation of aspirin and clopidogrel. The two compounds we will be preparing, aspirin acetylsalicylic acid and oil of wintergreen methyl salicylate, are both organic esters. It is a derivative of salicylic acid which is also an. Aspirin, a drug widely known for its analgesic, antipyretic, and antiinflammatory properties, is a compound derived from two acids namely acetic acid and salicylic acid. Pdf analytical method development and validation for aspirin. Novel application of hydrotropic solubilizing additives in. The reaction that is used for the synthesis is shown below. For the synthesis of aspirin, how do you calculate the percent yield if the reaction produces 4. Preparation of aspirin experiment 5 introduction in this experiment you will prepare a sample of aspirin, recrystallize the raw product, and determine the percentage yield of the aspirin based on the limiting reactant. Your team is employed by the generic pharmaceutical corp. Du journal of undergraduate research and innovation quantitative estimation of aspirin in various drugs. Synthesis of aspirin lab report and analysis odinity. Nov 15, 2009 if youre talking about the recrystallization, the wrong temperatures can result in impure product, loss of product, and oiling out. Aspirin sample essay sample sample essays online library.
Learn aspirin synthesis with free interactive flashcards. Please sign in to view account pricing and product availability. The purpose of this experiment is to synthesize aspirin acetyl salicylic acid from salicylic acid and acetic anhydride. Results and conclusion for aspirin synthesis essay. We use cookies to give you the best experience possible. Synthesis of aspirin ryan and jose 021214 abstract. Telea, an image inpainting technique based on the fast marching method, proc. Pdf aspirin acetylsalicylic acid, asa has been used as one of the most well known.
Recall that last week you did the reaction shown to prepare aspirin. Hplc2,3,4,5,6, spectrophotometric7, rphplc8,9, rp sequential injection chromatographyrpsic10. An improved depth map estimation for coding and view synthesis. This paper is an attempt to deliver goodquality depth estimation reference software ders that. View lab report aspirin lab from chem 053 at university of pennsylvania. Synthesis and spectral analysis of aspirin free essays.
Further, your team is to analyze the product for salicylic acid in a controlled, quantitative procedure, if possible. This figure mainly reflects purchase of 16,000 tons of aspirin tablets or 80 million tablets a year. Even so, to be able to analyse the composition of an aspirin sample or the amount of acetylsalicylic acid, the hydrolysis of the sample by alkali into neutrality is required. An ester is a compound that is formed when an acid containing the cooh group reacts with an alcohol a compound containing an oh group. This thesis is to study depth estimation reference software ders of. Chemistry 51 experiment 11 synthesis and analysis of aspirin. Hole filling method using depth based inpainting for view. Begin by rinsing the conical vial with acetone and assembling the heating apparatus. Transfer the two aspirin pieces into two 125 ml erlenmeyer flasks, and label the flasks sample 1 and sample 2. Aspirin synthesis tap water was heated on a steam bath in a 250 ml beaker. Another is measuring the melting point of the aspirin sample, which will in turn indicate the purity of the sample. Pdf enhanced view synthesis reference software vsrs. One of the most consumed drugs production in the us is 10 million.
This, however, has side goals that go along with the main one. Be sure to consult the procedure for the detailed instructions. Aug 08, 2016 synthesis of aspirin lab report essay example for free newyorkessays database with more than 65000 college essays for studying. Basically, sulfuric acid is used as an acid catalyst. Finally, a multilateral filtering is used to preserve details in the depth map and simultaneously smooth the depths in occluded areas at object boundary, less texture and discontinuity regions. M tanimoto, t fujii, k suzuki, n fukushima, y mori. Environmental education resources to commemorate earth days 50th anniversary. Uv vis absorption spectroscopy and colorimetric studies. For the synthesis of aspirin, how do you calculate the. By continuing well assume youre on board with our cookie policy.
We will attempt to purify the aspirin via recrystallization with ethanol. It has the ability to reduce fever an antipyretic, to reduce pain an analgesic, and to reduce swelling, soreness, and redness an antiinflammatory agent. Synthesis and characterization of aspirin chemistry m01b lab 07 97 crystals dry for a few minutes before weighing them. Formulation and evaluation of aspirin delayed release tablet. Accuracy of the method was indicated by recovery values of aspirin and clopidogrel were 99.
Below are many of the experimental steps you will perform in this lab. Since they require a huge number of pixels for a rich immersive media, an efficient data compression method is essential. Easy and precise methods were developed for estimation of aspirin asp. Du journal of undergraduate research and innovation. Record the temperature of the melting point range temperature of your. General chemistry laboratory experiments, suzanne w slayden, 1999, 3rd edition, pages 5766. In this paper, we propose the depth estimation and view synthesis approaches for the scene rendering of narrowbaseline videos. Quantitative determination of acetylsalicylic acid in. Aspirin synthesis lab quiz honors chemistry 2 with. View data points was selected in the toolbar, which showed the wavenumber. This week you will use nmr, ir, and melting point to characterize your product. May 05, 20 aspirin, a drug widely known for its analgesic, antipyretic, and antiinflammatory properties, is a compound derived from two acids namely acetic acid and salicylic acid. Depth imagebased virtual view synthesis the threedimensional image warping 3d warping is a key technique in depthbased view synthesis.
Synthesis and analysis of aspirin lab flashcards quizlet. This document presents results of experiments performed with depth estimation and view synthesis software, kindly provided by nagoya university 1. Aspirin and acetic acid are formed when the hydrogen in the phenolic alcohol group of salicylic acid is replaced by an acetyl h3ccoo group. You have been asked to evaluate a simple organic synthesis for aspirin and to determine if the synthesis merits further funding by santa monica pharmaceuticals. Furthermore, the other objectives were to enable students to conduct the synthesis of aspirin, reinforce skills or recrystallisation and the technique of melting point determination. Aspirin synthesis your team of scientists has been hired by the drug research division of santa monica pharmaceuticals, a new startup company formed by some smc alumni. It happens when a carboxylic acid from the salicylic acid and an alcohol combine in a reaction therefore producing an ester. View notes aspirin synthesis and characterization lab report from chem 151 at university of arizona. Experiment 22 synthesis of aspirin and oil of wintergreen. The amount of each compound should be the same because there is a 1.
Suzuki, reference software of depth estimation and view synthesis for ftv3dv, isoiec jtc1sc29wg11, m15836, october 2008. The purpose of this experiment is to create aspirin by reacting salicylic acid with acetic anhydride. Your job is to find and test a synthesis procedure for acetylsalicylic acid aspirin. Aspirin is used medically to reduce fever and pain. Performs the synthesis of acetylsalicylic acid aspirin purification by recrystallization and using melting point to confirm identity. Aspirin is one of the milder and least expensive pain relievers available. Spectroscopic estimation of calibration curve of liposome carrying aspirin. Results of analysis by proposed method and phamacopoeial method are very comparable. Study 10 aspirin synthesis lab quiz flashcards from brittni t. Allow these solutions to cool, and then transfer then into. Aspirinmediated attenuation of intervertebral disc degeneration by. Aspirin synthesis lab report by eddie zhang on prezi. Both of these specify range of disparity values for which image correspondence is sought. The balanced chemical reaction of the formation of aspirin.
Synthesis of aspirin, purification and analysis using tlc. The synthesis and characterization of aspirin part 1 purpose. Aspirin acetylsalicylic acid is an important antiinflammatory and analgesicpyretic drug. Synthesis of aspirin with a difference posted on april 7th, 2015 aspirin is a pain relieving compound that most students will be familiar with, thus its synthesis gives students an insight into how chemistry is used in reallife applications. Mar 19, 2015 synthesis and spectral analysis of aspirin by. Salicylic acid was first discovered in the bark of willow tree. German chemist felix hoffmann synthesized what would become known as. This paper is an attempt to deliver goodquality depth estimation reference software ders that is wellstructured for further use in the worldwide mpeg standardization committee. A09009a determination of aspirin using uv and visible wa. The specific nucleophilic acyl substitution for this experiment is esterification. Synthesis and characterization of aspirin chemistry m01b lab 07 96 the aspirin you will prepare in this experiment is somewhat impure and should certainly not be taken internally, even if the experiment gives you a bad headache. The synthesis of aspirin involved the acidcatalyzed nuclephilic acyl substitution. Synthesis and analysis of acetyl salicylic acid amy chan chem 290 section 1 november 25, 2002.
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